Maitiro eSynthesis aTantalum Pentachloridekunyanya inosanganisira inotevera nhanho:
1, kugadzirira kwezvinhu
Gadzirira yakakwirira-yekuchenaTantalum simbiuye yakakwirira-yakanyanya chlorine kana hydrogen chloride (HCL) seyakagadzirwa zvinhu. Kuchena kweTantalumsimbiine kukosha kwakakosha pakuchena kwechigadzirwa chekupedzisira.
2, chlorination reaction
Direct chlorination nzira: Tantalum simbi yakatemwa kana powra, uye yakabva yaiswa mune yeklorine gasi rwizi rweClorination reaction pane tembiricha yegumi nemazana 170-250. Chlorine gasi inobata ne tantalum kuburitsa tantalum pentachloride. Kuita uku kunogona kuitwawo uchishandisa HCL, asi kunoda kuitwa pakudziya kwakanyanya (senge 400).
Indiirect Clllination nzira: Tantalum Pentachloride inogona zvakare kuwanikwa nekuita tantalum pentoxide neTiiryl
Ta2o5 + 5 Socll2 → 2 Tacl5 + 5 So2.
3, kupatsanurana uye kucheneswa
Kutonhorera gasi kunogadzirwa neiyo korlinisation maitiro ekuzvinyaradza mumvura.
Kuparadzanisa uye simbisa mvura tantalum pentachloride kubva pakusvibiswa. Kazhinji, distillation uye dzimwe nzira dzinoshandiswa kuparadzanisa zvakasarudzika zvakasarudzika zvichienderana nemisiyano yavo yekubikira. Iyi nhanho yakakosha kuti uone kuchena kweTantalum Pentachloride.
4, kuomesa kurapwa
Pukuta akapatsanurwa uye akanatswaTantalum Pentachloridekubvisa kumusoro kwemukati uye kusachena. Kuomesa kurapwa kwakakosha kuchengetedza kugadzikana uye kuchena kweTantalum Pentachloride.
Kutumira Nguva: Sep-05-2020